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In this seminar, I will describe our recent work in two areas: (a) the rational design of molybdenum-based catalysts inspired by biological C\u2013H hydroxylases, and (b) the exploration of aluminum(II) chemistry for small molecule activation.\n\nIn the first part, I will outline our efforts to develop structural and functional mimics of Mo-dependent hydroxylases such as xanthine oxidase and ethylbenzene dehydrogenase. These studies aim to generate catalysts that can hydroxylate C\u2013H bonds in complex molecules with complementary site selectivity to existing technologies.\n\nIn the second part, I will highlight our discovery of Al\u2013Fe bond homolysis in heterobimetallic complexes as a route to Al-based radicals\u2014formally Al(II) species\u2014that exploit strain-induced biphilicity or redox non-innocence. These properties enable new pathways for small molecule activation. 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